1
Department of Chemistry, Faculty of Science, University of Guilan
2
Department of Chemistry, Faculty of Science, University o f Mohaghegh Ardabili
3
Department of Chemistry, Faculty of Science, University o f Mohaghegh Ardabili, Ardabil
Abstract
In this research, cobalt and nickel sulfide nanoparticles (NPs) were grown on AlMCM-41 matrix by using ion exchange method. The prepared samples were irradiated by thermalized neutron that emitted from Am-Be source up to fluencies (7.9+E9n/cm2). After that, X-ray diffraction (XRD), UV-Vis spectroscopy, Fourier transform infrared (FTIR), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were used for irradiated and non-irradiated samples characterization. The results show nanoparticles aggregation in NiS/AlMCM-41 is more than CoS/AlMCM-41 sample. The TEM images show average size of CoS NPs before and after neutron radiation about 20 and 50 nm, respectively. In this way, average size of NiS anoparticles before and after neutron radiation 130 and 70 nm respectively. The DRS results show that Co2+ and Ni2+ ions produced after neutron radiation, located in tetrahedral sites in AlMCM-41. The results indicate host materials have important role in decrease of radiation defects (RDs).
Sohrabnezhad*,S. , Rezaei Ochbelgh,D. and Morsali Golboos,N. (2013). Irradiation with Neutrons and Formation of Simple Radiation Defects in Semiconductors. International Journal of Nanoscience and Nanotechnology, 9(2), 61-70.
MLA
Sohrabnezhad*,S. , , Rezaei Ochbelgh,D. , and Morsali Golboos,N. . "Irradiation with Neutrons and Formation of Simple Radiation Defects in Semiconductors", International Journal of Nanoscience and Nanotechnology, 9, 2, 2013, 61-70.
HARVARD
Sohrabnezhad* S., Rezaei Ochbelgh D., Morsali Golboos N. (2013). 'Irradiation with Neutrons and Formation of Simple Radiation Defects in Semiconductors', International Journal of Nanoscience and Nanotechnology, 9(2), pp. 61-70.
CHICAGO
S. Sohrabnezhad*, D. Rezaei Ochbelgh and N. Morsali Golboos, "Irradiation with Neutrons and Formation of Simple Radiation Defects in Semiconductors," International Journal of Nanoscience and Nanotechnology, 9 2 (2013): 61-70,
VANCOUVER
Sohrabnezhad* S., Rezaei Ochbelgh D., Morsali Golboos N. Irradiation with Neutrons and Formation of Simple Radiation Defects in Semiconductors. International Journal of Nanoscience and Nanotechnology, 2013; 9(2): 61-70.
